C₂₁H₃₃NO₂

Base Information

Chemical Name:C₂₁H₃₃NO₂
CAS No.:1430811-63-4
Molecular Formula:C₂₁H₃₃NO₂
Molecular Weight:331.499
Hs Code.:

C<sub>21</sub>H<sub>33</sub>NO<sub>2</sub>

Synonyms:C₂₁H₃₃NO₂

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Chemical Property of C₂₁H₃₃NO₂

Chemical Property:

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Technology Process of C₂₁H₃₃NO₂

There total 7 articles about C₂₁H₃₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1430811-73-6
(S)-5-(4-octylphenethyl)-5-azido-5,6-dihydropyran-2-one

: 1430811-63-4
C₂₁H₃₃NO₂

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃;
DOI:10.1016/j.bmc.2013.02.042

Reference yield:

: 49763-66-8
4-octylbenzaldehyde

: 1430811-63-4
C₂₁H₃₃NO₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide / tetrahydrofuran; water / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 3 h / 60 °C / Inert atmosphere

4.1: hydrogenchloride; water / methanol / 1 h / 20 °C / Inert atmosphere

5.1: titanium(IV) isopropylate; D-(-)-diisopropyl tartrate / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

6.1: potassium carbonate / water; isopropyl alcohol / 0 - 20 °C / Inert atmosphere

7.1: diisopropoxytitanium diazide / toluene / 0.25 h / 85 °C / Inert atmosphere

8.1: hydrogen; palladium 10% on activated carbon / ethanol / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; n-butyllithium; diisopropoxytitanium diazide; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; D-(-)-diisopropyl tartrate; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water; isopropyl alcohol; toluene; 1.2: |Wittig Olefination / 3.2: |Suzuki Coupling / 5.1: |Sharpless Asymmetric Epoxidation / 5.2: |Dess-Martin Oxidation / 6.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.bmc.2013.02.042

Reference yield:

: 46745-66-8
1-octyl-4-vinylbenzene

: 1430811-63-4
C₂₁H₃₃NO₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; water / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 60 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol / 1 h / 20 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; D-(-)-diisopropyl tartrate / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

5.1: water; isopropyl alcohol / Inert atmosphere

6.1: diisopropoxytitanium diazide / toluene / 0.25 h / 85 °C / Inert atmosphere

7.1: hydrogen; palladium 10% on activated carbon / ethanol / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; diisopropoxytitanium diazide; palladium 10% on activated carbon; water; hydrogen; D-(-)-diisopropyl tartrate; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water; isopropyl alcohol; toluene; 2.2: |Suzuki Coupling / 4.1: |Sharpless Asymmetric Epoxidation / 4.2: |Dess-Martin Oxidation / 5.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.bmc.2013.02.042