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dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate

Base Information Edit
  • Chemical Name:dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate
  • CAS No.:742101-73-1
  • Molecular Formula:C20H18O7
  • Molecular Weight:370.359
  • Hs Code.:
  • Mol file:742101-73-1.mol
dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate

Synonyms:dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate

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Chemical Property of dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate Edit
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Technology Process of dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate

There total 8 articles about dimethyl 5-[3-(2-hydroxy-5-methylphenyl)-3-oxopropanoyl]isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 5 steps
1: 84 percent / K2CO3 / dimethylformamide / 14 h / 40 °C
2: 49 percent / LiOH / tetrahydrofuran; H2O / 2.5 h / 20 °C
3: SOCl2; DMF / Heating
4: 58 percent / pyridine / 0.5 h / 50 °C
5: 59 percent / pyridine; KOH / 1.5 h / 50 °C
With pyridine; potassium hydroxide; lithium hydroxide; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; water; N,N-dimethyl-formamide; 4: Schotten-Baumann reaction / 5: Baker Venkataraman rearrangement;
DOI:10.1021/jm020839k
Guidance literature:
Multi-step reaction with 4 steps
1: 49 percent / LiOH / tetrahydrofuran; H2O / 2.5 h / 20 °C
2: SOCl2; DMF / Heating
3: 58 percent / pyridine / 0.5 h / 50 °C
4: 59 percent / pyridine; KOH / 1.5 h / 50 °C
With pyridine; potassium hydroxide; lithium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; water; 3: Schotten-Baumann reaction / 4: Baker Venkataraman rearrangement;
DOI:10.1021/jm020839k
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