1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

Base Information

Chemical Name:1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate
CAS No.:742101-61-7
Molecular Formula:C₂₀H₁₈O₇
Molecular Weight:370.359
Hs Code.:

Synonyms:1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

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Chemical Property of 1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

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Technology Process of 1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

There total 6 articles about 1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1450-72-2
5-methyl-2-hydroxyacetophenone

: 68872-14-0
dimethyl 5-(chlorocarbonyl)benzene-1,3-dioate

: 742101-61-7
1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

Guidance literature:: With pyridine; at 50 ℃; for 0.5h;
DOI:10.1021/jm020839k

Reference yield:

: 554-95-0
benzene-1,3,5-tricarboxylic acid

: 742101-61-7
1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / K₂CO₃ / dimethylformamide / 14 h / 40 °C

2: 49 percent / LiOH / tetrahydrofuran; H₂O / 2.5 h / 20 °C

3: SOCl₂; DMF / Heating

4: 58 percent / pyridine / 0.5 h / 50 °C

With pyridine; lithium hydroxide; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; water; N,N-dimethyl-formamide; 4: Schotten-Baumann reaction;
DOI:10.1021/jm020839k

Reference yield:

: 2672-58-4
1,3,5-tris-(methoxycarbonyl)benzene

: 742101-61-7
1-(2-acetyl-4-methylphenyl) 3,5-dimethyl benzene-1,3,5-tricarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / LiOH / tetrahydrofuran; H₂O / 2.5 h / 20 °C

2: SOCl₂; DMF / Heating

3: 58 percent / pyridine / 0.5 h / 50 °C

With pyridine; lithium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; water; 3: Schotten-Baumann reaction;
DOI:10.1021/jm020839k