2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

Base Information

Chemical Name:2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole
CAS No.:79047-57-7
Molecular Formula:C₁₅H₁₈ClN₃O₃
Molecular Weight:323.779
Hs Code.:

Synonyms:2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

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Chemical Property of 2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

Chemical Property:

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Technology Process of 2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

There total 1 articles about 2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79047-41-9
2-n-butyl-4-chloro-5-hydroxymethylimidazole

: 3958-60-9
2-nitrophenylmethyl bromide

: 2-n-butyl-5-chloro-4-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

: 79047-57-7
2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

Guidance literature:: With sodium methylate; Multistep reaction; 1.) methanol, 0 deg C, 2.) DMF, 25 deg C;
DOI:10.1021/jm00167a007

Reference yield:

: 79047-57-7
2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

: 2-Butyl-4-chloro-5-chloromethyl-1-(2-nitro-benzyl)-1H-imidazole

Guidance literature:: With thionyl chloride; In chloroform; at 0 - 20 ℃; for 2h;
DOI:10.1021/jm00167a007

Reference yield:

: 79047-57-7
2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-nitrophenyl)methyl>imidazole

: 123632-62-2
EXP 6026

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / CHCl₃ / 2 h / 0 - 20 °C

2: dimethylsulfoxide

3: 12 N HCl, glacial acetic acid / 6 h / Heating

4: 3.1 M HCl / dioxane / 7.5 h / Heating

With hydrogenchloride; thionyl chloride; acetic acid; In 1,4-dioxane; chloroform; dimethyl sulfoxide;
DOI:10.1021/jm00167a007