N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester

Base Information

Chemical Name:N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester
CAS No.:83241-78-5
Molecular Formula:C₂₃H₁₉NO₂S
Molecular Weight:373.475
Hs Code.:

Synonyms:N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester

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Technology Process of N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester

There total 2 articles about N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 83251-66-5
N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester; compound with perchloric acid

: 83241-78-5
N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester

Guidance literature:: With potassium carbonate; In acetone;
DOI:10.1016/0040-4020(82)85072-2

Reference yield:

: 15724-87-5
p-methoxyphenyl β-chlorovinyl ketone

: 636-04-4
N-Phenylbenzothioamide

: 83241-84-3
N-[(E)-3-(4-Methoxy-phenyl)-3-oxo-propenyl]-N-phenyl-thiobenzamide

: 83241-78-5
N-Phenyl-thiobenzimidic acid (Z)-3-(4-methoxy-phenyl)-3-oxo-propenyl ester

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) ether, n-hexane, -40/-50 deg C, 2) ether, -40/-50 deg C, 1 h; -10 deg C, 2 h; room temp., 4 h;
DOI:10.1016/0040-4020(82)85072-2