(E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine

Base Information

• Chemical Name: (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine
• CAS No.: 74904-68-0
• Molecular Formula: C₂₁H₂₇NO₅
• Molecular Weight: 373.449

Synonyms:(E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine

Chemical Property of (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine

Chemical Property:

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Technology Process of (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine

There total 2 articles about (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

cis-(+/-)laudanosine N-oxide (74904-62-4,74904-66-8,81872-02-8,106488-66-8,112531-10-9,112531-11-0) → (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine (74904-68-0) + (3RS,3aRS,8aSR)-3-(3,4-dimethoxyphenyl)-5,6-dimethoxy-1-methyl-3,3a,8,8a-tetrahydro-1H-inden<2,1-c>isoxazole (74904-75-9) + 1-(3,4-dimethoxybenzyl)-7,8-dimethoxy-3-methyl-1,3,4,5-tetrahydro-2,3-benzoxazepine (74904-73-7) + (1RS,2RS,4RS)-2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydro-2H-1,4-methano-4H-3,4-benzoxazocine (74904-74-8) + laudanosine (1699-51-0,20412-65-1)

Guidance literature:

at 150 ℃; for 0.5h; Product distribution; Mechanism; other laudanosine N-oxides;

DOI:10.1071/CH9800379c

Reference yield: 9.0%

cis-(+/-)laudanosine N-oxide (74904-62-4,74904-66-8,81872-02-8,106488-66-8,112531-10-9,112531-11-0) → (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine (74904-68-0) + (3RS,3aRS,8aSR)-3-(3,4-dimethoxyphenyl)-5,6-dimethoxy-1-methyl-3,3a,8,8a-tetrahydro-1H-inden<2,1-c>isoxazole (74904-75-9) + 1-(3,4-dimethoxybenzyl)-7,8-dimethoxy-3-methyl-1,3,4,5-tetrahydro-2,3-benzoxazepine (74904-73-7) + (1RS,2RS,4RS)-2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydro-2H-1,4-methano-4H-3,4-benzoxazocine (74904-74-8)

Guidance literature:

at 150 ℃; for 0.5h;

DOI:10.1071/CH9800379c

Reference yield: 83.0%

chloroformic acid ethyl ester (541-41-3) + (E)-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-N-methylhydroxylamine (74904-68-0) → (E)-O-acetyl-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-O-ethoxycarbonyl-N-methylhydroxylamine (74904-70-4)

Guidance literature:

With pyridine; In benzene; for 2h; Heating;

DOI:10.1071/CH9800379c

upstream raw materials:

cis-(+/-)laudanosine N-oxide

Downstream raw materials:

(E)-O-acetyl-N-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>ethyl-O-ethoxycarbonyl-N-methylhydroxylamine

(E)-2-<2-<2-(3,4-dimethoxyphenyl)ethenyl>-4,5-dimethoxyphenyl>-N-methylethanamine

(3RS,3aRS,8aSR)-3-(3,4-dimethoxyphenyl)-5,6-dimethoxy-1-methyl-3,3a,8,8a-tetrahydro-1H-inden<2,1-c>isoxazole

(1RS,2RS,4RS)-2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydro-2H-1,4-methano-4H-3,4-benzoxazocine

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