aquahydridohydroxobis(triphenylphosphine)ruthenium(II)

Base Information

Chemical Name:aquahydridohydroxobis(triphenylphosphine)ruthenium(II)
CAS No.:63827-91-8
Molecular Formula:C₃₆H₃₄O₂P₂Ru
Molecular Weight:661.682
Hs Code.:

Synonyms:aquahydridohydroxobis(triphenylphosphine)ruthenium(II)

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Chemical Property of aquahydridohydroxobis(triphenylphosphine)ruthenium(II)

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Technology Process of aquahydridohydroxobis(triphenylphosphine)ruthenium(II)

There total 4 articles about aquahydridohydroxobis(triphenylphosphine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 55102-19-7,879374-40-0,879374-44-4,99944-74-8
chlorohydridotris(triphenylphosphine)ruthenium(II)

: 63827-91-8
aquahydridohydroxobis(triphenylphosphine)ruthenium(II)

Guidance literature:: With potassium hydroxide; water; In water; toluene; Ar-atmosphere; stirring of Ru-complex and KOH in mixt. of H2O and toluene (1/1 v/v) overnight; collection, washing (H2O), drying (vac.);
DOI:10.1039/DT9770001546

Reference yield: 50.0%

: 55102-19-7,879374-40-0,879374-44-4,99944-74-8
chlorohydridotris(triphenylphosphine)ruthenium(II)

: diμ-hydroxo-bis[acetonehydridobis(triphenylphosphine)ruthenium(II)]

: Ru₄H₄(OH)2(P(C₆H₅)2)2(CO)2(P(C₆H₅)3)6((CH₃)2CO)2

: 63827-91-8
aquahydridohydroxobis(triphenylphosphine)ruthenium(II)

Guidance literature:: With potassium hydroxide; water; In water; acetone; byproducts: benzene; Ar-atmosphere; refluxing in Me2CO contg. water (3 h); filtration off of RuH(OH)(PPh3)2(H2O), volume reduction, addn. of light petroleum, filtration off of (RuH(OH)(PPh3)2(Me2CO))2, crystn. on addn. of light petroleum to filtrate and cooling, collection, washing (light petroleum), drying (vac.); elem. anal.;
DOI:10.1039/DT9770001546