3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

Base Information

Chemical Name:3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole
CAS No.:1179326-76-1
Molecular Formula:C₄₃H₃₄N₂O₁₀
Molecular Weight:738.75
Hs Code.:

Synonyms:3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

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Chemical Property of 3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

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Technology Process of 3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

There total 1 articles about 3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 36288-37-6
N-hydroxy-4-methylbenzenecarboximidoyl chloride

: 286369-05-9
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl cyanide

: 1179326-76-1
3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

Guidance literature:: N-hydroxy-4-methylbenzenecarboximidoyl chloride; 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl cyanide; In toluene; at 110 ℃; Inert atmosphere;

With triethylamine; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2009.04.036

Reference yield: 92.0%

: 1179326-76-1
3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

: 1179326-90-9
5-(2-deoxy-D-arabino-hex-1-enopyranosyl)-3-(4-methoxyphenyl)-1,2,4-oxadiazole

: 1179326-82-9
5-(β-D-glucopyranosyl)-3-(4-methylphenyl)-1,2,4-oxadiazole

Guidance literature:: 3-(4-methylphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole; With sodium methylate; In methanol; at 20 ℃; for 3h;

With Dowex 50Wx₂; In methanol; pH=5;
DOI:10.1016/j.bmc.2009.04.036