Technology Process of C24H40O3S
There total 7 articles about C24H40O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: CH3CH2COOH / 145 °C
2: LiBH4 / methanol
3: 97 percent / sodium; hexamethylphosphoramide / 2-methyl-propan-2-ol
4: 89 percent / triethylamine; 4-(dimethylamino)pyridine / CH2Cl2
5: NaI / butan-2-one / Heating
6: dimethylformamide / 70 °C
7: 85 percent / HBF4 / methanol; H2O
With
N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium borohydride; tetrafluoroboric acid; sodium; propionic acid; triethylamine; sodium iodide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;
DOI:10.1002/anie.200603853
- Guidance literature:
-
Multi-step reaction with 6 steps
1: LiBH4 / methanol
2: 97 percent / sodium; hexamethylphosphoramide / 2-methyl-propan-2-ol
3: 89 percent / triethylamine; 4-(dimethylamino)pyridine / CH2Cl2
4: NaI / butan-2-one / Heating
5: dimethylformamide / 70 °C
6: 85 percent / HBF4 / methanol; H2O
With
N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium borohydride; tetrafluoroboric acid; sodium; triethylamine; sodium iodide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;
DOI:10.1002/anie.200603853