(E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene

Base Information

• Chemical Name: (E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene
• CAS No.: 1155867-61-0
• Molecular Formula: C₂₁H₂₈OSi
• Molecular Weight: 324.538
• Mol file: 1155867-61-0.mol

Synonyms:(E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene

Chemical Property of (E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene

Chemical Property:

Purity/Quality:

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Technology Process of (E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene

There total 1 articles about (E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(E)-3-(2-hydroxyphenyl)-1-phenylpropene (23925-16-8) + tert-butyldimethylsilyl chloride (18162-48-6) → (E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene (1155867-61-0)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1055/s-0028-1083361

Reference yield: 89.0%

(E)-1-phenyl-3-[2-(tert-butyldimethylsilyloxy)phenyl]propene (1155867-61-0) → (1S,2S)-1-phenyl-3-[2-(tertbutyldimethylsilyloxy)phenyl]propane-1,2-diol (1155867-62-1)

Guidance literature:

With methanesulfonamide; AD-mix-α; In chloroform; water; tert-butyl alcohol; at 20 ℃; for 16h; enantioselective reaction;

DOI:10.1055/s-0028-1083361

upstream raw materials:

(E)-3-(2-hydroxyphenyl)-1-phenylpropene

tert-butyldimethylsilyl chloride

Downstream raw materials:

(1S,2S)-1-phenyl-3-[2-(tertbutyldimethylsilyloxy)phenyl]propane-1,2-diol