Technology Process of C22H23NO5S
There total 3 articles about C22H23NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl-ammonium chloride; palladium diacetate;
In
N,N-dimethyl-formamide;
for 3h;
Inert atmosphere;
Reflux;
DOI:10.1021/ol501078d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / tetrachloromethane / 1 h / Inert atmosphere; Reflux
2: potassium hydroxide / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere
3: palladium diacetate; tetrabutyl-ammonium chloride / N,N-dimethyl-formamide / 3 h / Inert atmosphere; Reflux
With
N-Bromosuccinimide; tetrabutyl-ammonium chloride; palladium diacetate; potassium hydroxide;
In
tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol501078d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere
2: palladium diacetate; tetrabutyl-ammonium chloride / N,N-dimethyl-formamide / 3 h / Inert atmosphere; Reflux
With
tetrabutyl-ammonium chloride; palladium diacetate; potassium hydroxide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol501078d