methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate

Base Information

Chemical Name:methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate
CAS No.:83152-64-1
Molecular Formula:C₂₀H₂₈N₂O₃
Molecular Weight:344.454
Hs Code.:

Synonyms:methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate

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Chemical Property of methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate

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Technology Process of methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate

There total 2 articles about methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 83152-59-4
(5R,6S,7R)-7-Diethylcarbamoyl-5,7-dimethyl-6-phenyl-2-oxa-1-aza-bicyclo[3.2.0]hept-3-ene-4-carboxylic acid methyl ester

: 83152-64-1
methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 40h; under 760 Torr;
DOI:10.1021/jo00144a005

Reference yield:

: 75909-31-8
N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide

: 83152-64-1
methyl 6-<(diethylamino)carbonyl>-1,4,5,6-tetrahydro-4,6-dimethyl-5-phenyl-3-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / CH₂Cl₂ / 24 h / Heating

2: 78 percent / H₂ / 5percent Pd on charcoal / ethanol / 40 h / 760 Torr

With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo00144a005