(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

Base Information

Chemical Name:(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride
CAS No.:1450837-89-4
Molecular Formula:C₁₆H₂₃N₃O₂S*ClH
Molecular Weight:357.904
Hs Code.:

Synonyms:(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

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Technology Process of (2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

There total 1 articles about (2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1450837-84-9
(2S)-2-tert-butyl 6-ethanethioamido-1-oxo-1-(2-oxo-2-phenylethylamino)hexan-2-ylcarbamate

: 1450837-89-4
(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

Guidance literature:: With hydrogenchloride; ethane-1,2-dithiol; In water; isopropyl alcohol; at 60 ℃; for 2h;
DOI:10.1021/jm400438k

Reference yield: 23.0%

: 1450837-89-4
(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

: 13504-85-3
(2S,4R)-1-(benzyloxycarbonyl)-4-hydroxypyrrolidine-2-carboxylic acid

: (2S,4R)-N-[(2S)-6-ethanethioylamino-1-(2-oxo-2-phenylethylamino)-1-oxohexan-2-yl]-4-hydroxypyrrolidine-1-benzyloxycarbonyl-2-carboxamide

Guidance literature:: (2S,4R)-1-(benzyloxycarbonyl)-4-hydroxypyrrolidine-2-carboxylic acid; With pyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jm400438k

Reference yield: 23.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1450837-89-4
(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride

: (2S)-N-[(2S)-6-ethanethioylamino-1-(2-oxo-2-phenylethylamino)-1-oxohexan-2-yl]-pyrrolidine-1-tert-butoxycarbonyl-2-carboxamide

Guidance literature:: 1-(tert-butoxycarbonyl)-L-proline; With pyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

(2S)-2-amino-6-ethanethioylamino-N-(2-oxo-2-phenylethyl)hexanamide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jm400438k