2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate
CAS No.:912628-03-6
Molecular Formula:C₂₃H₂₉NO₁₀S
Molecular Weight:516.51
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

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Chemical Property of 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

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Technology Process of 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

There total 7 articles about 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 19879-84-6
tetraacetyl thioglucose

: (E)-[2H₅]hydrocinnamaldehyde oximyl chloride

: 912628-03-6
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1002/jlcr.1225

Reference yield:

: 4165-57-5
bromobenzene-d5

: 912628-03-6
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

Guidance literature:: Multi-step reaction with 5 steps

1.1: Mg; CuBr / tetrahydrofuran

1.2: 100 percent / tetrahydrofuran

2.1: 93 percent / HCl / H₂O; acetone

3.1: 88 percent / NH₂OH*HCl; NaOAc / ethanol / Heating

4.1: 82 percent / N-chlorosuccinimide; pyridine / CHCl₃

5.1: 74 percent / Et₃N / tetrahydrofuran

With pyridine; hydrogenchloride; N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; magnesium; triethylamine; copper(I) bromide; In tetrahydrofuran; ethanol; chloroform; water; acetone;
DOI:10.1002/jlcr.1225

Reference yield:

: 253305-66-7
[2H₅]hydrocinnamaldehyde

: 912628-03-6
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-1-[phenyl-2H5]phenylethyl thiohydroximate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NH₂OH*HCl; NaOAc / ethanol / Heating

2: 82 percent / N-chlorosuccinimide; pyridine / CHCl₃

3: 74 percent / Et₃N / tetrahydrofuran

With pyridine; N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; triethylamine; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1002/jlcr.1225