Technology Process of C43H54N8O7
There total 11 articles about C43H54N8O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C39H48N6O5;
With
hydrogenchloride;
In
1,4-dioxane; dichloromethane;
for 0.333333h;
N-methoxycarbonyl-L-valine;
With
N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / acetonitrile / 20 °C
2.1: ammonium acetate / toluene / 14 h / 100 °C
3.1: potassium acetate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 14 h / 80 °C / Inert atmosphere
4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 2 h / 95 °C / Inert atmosphere
5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0.33 h
5.2: 1 h / 20 °C
With
hydrogenchloride; ammonium acetate; potassium acetate; sodium hydrogencarbonate; triethylamine;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium acetate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 14 h / 80 °C / Inert atmosphere
2.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 2 h / 95 °C / Inert atmosphere
3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0.33 h
3.2: 1 h / 20 °C
With
hydrogenchloride; potassium acetate; sodium hydrogencarbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water;