((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten⁽⁰⁾

Base Information

• Chemical Name: ((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten⁽⁰⁾
• CAS No.: 38669-74-8
• Molecular Formula: C₁₃H₇ClO₆W
• Molecular Weight: 478.498

Synonyms:((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten⁽⁰⁾

Chemical Property of ((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten⁽⁰⁾

Chemical Property:

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Technology Process of ((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten⁽⁰⁾

There total 1 articles about ((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((4-chlorophenyl)methoxy(propargyloxy)methyl)pentacarbonyltungsten(1-) → ((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten(0) (38669-74-8)

Guidance literature:

With triethylamine; In water; acetonitrile; freshly generated soln. of the complex in CH3CN was added to aq. soln. of N(C2H5)3 buffer (pH 10.5) in a stopped-flow spectrophotometer at 25°C; monitoring around 400 nm; Kinetics;

DOI:10.1021/ja994174w

Reference yield:

((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten(0) (38669-74-8) + sodium methylate (124-41-4) → (dimethoxy(4-chlorophenyl)methyl)pentacarbonyltungsten(1-)

Guidance literature:

In methanol; soln. of the complex in CH3OH (the stability of the soln. could be enhanced by adding CH3SO3H 2.5E-3 M) was mixed with NaOCH3 (soln. in CH3OH) in a stopped-flow spectrophotometer at 25°C; monitoring around 400 nm; Kinetics;

DOI:10.1021/ja994174w

Reference yield:

((4-chlorophenyl)methoxycarbene)pentacarbonyltungsten(0) (38669-74-8) → (OC)5WC(C6H4Cl)(SCH2CH2OH)2(1-)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene; methanol

2: water; acetonitrile

In methanol; water; acetonitrile; benzene;

DOI:10.1021/ja992741+

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