silver derivative of N,N'-di-p-tolylformamidine

Base Information

Chemical Name:silver derivative of N,N'-di-p-tolylformamidine
CAS No.:65585-77-5
Molecular Formula:Ag*C₁₅H₁₅N₂
Molecular Weight:331.166
Hs Code.:

Synonyms:silver derivative of N,N'-di-p-tolylformamidine

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Chemical Property of silver derivative of N,N'-di-p-tolylformamidine

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Technology Process of silver derivative of N,N'-di-p-tolylformamidine

There total 1 articles about silver derivative of N,N'-di-p-tolylformamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: silver nitrate

: 16596-03-5,141417-88-1
N,N'-di-p-tolylformamidine

: 65585-77-5
silver derivative of N,N'-di-p-tolylformamidine

Guidance literature:: With ammonium hydroxide; In methanol; water; under Ar; aq. soln. of ammonium hydroxide added to soln. of ligand in MeOH; soln. of AgNO3 in H2O added with stirring; modified from S. J. Archibald et al., Inorg. Chem., 1999, 38, 5571; filtered; ppt. washed with MeOH; vac. dried in absence of light;
DOI:10.1021/om100740q

Reference yield: 90.0%

: 65585-77-5
silver derivative of N,N'-di-p-tolylformamidine

: 116722-41-9
Ag⁽¹⁺⁾*S₂C(CH₃C₆H₄)NCHN(C₆H₄CH₃)^(1-)=[Ag(S₂C(CH₃C₆H₄)NCHNC₆H₄CH₃)]

Guidance literature:: With carbon disulfide; In dichloromethane; CS2 added to soln. of (Ag(TolNCHNTol))n in CH2Cl2, stirred for 3 h; evapd., EtOH added, solid filtered off, washed with EtOH; elem. anal.;
DOI:10.1016/0022-328X(87)80102-X

Reference yield: 78.0%

: 65585-77-5
silver derivative of N,N'-di-p-tolylformamidine

: [Pd((C₆H₄)PPh₂)Br]₄

: 1289129-68-5
Pd₂[(C₆H₄)PPh₂]2[N,N'-di-p-tolylformamidinate]2

Guidance literature:: In dichloromethane; under Ar; Ag compd. added to suspn. of Pd complex in CH2Cl2; stirred in absence of light for 3 h; filtered; filtrate evapd. to dryness; dissolved in CH2Cl2; filtered overshort plug of silica; pptd. by addition of hexane; filtered; ppt. washe d with hexane; elem. anal.;
DOI:10.1021/om100740q