AKOS AU36-M72

Base Information

• Chemical Name: AKOS AU36-M72
• CAS No.: 16596-03-5
• Molecular Formula: C₁₅H₁₆N₂
• Molecular Weight: 224.305
• Hs Code.: 2925290090
• Mol file: 16596-03-5.mol

Synonyms:N,N'-Di-p-tolyl-formamidine;N,N'-Bis(4-methylphenyl)imidoformamide;N1,N2-Di-p-tolyl-formamidine;N,N'-di-(4-methyl)phenylformamidine;N,N'-bis(p-methylphenyl)formamidine;N,N'-bis(4-methylphenyl)formamidine;

Chemical Property of AKOS AU36-M72

Chemical Property:

• PSA: 24.39000
• LogP: 4.14830

Purity/Quality:

N,N'-DI(P-TOLYL)FORMAMIDINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS AU36-M72

There total 40 articles about AKOS AU36-M72 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

p-toluidine (106-49-0,12221-03-3) + orthoformic acid triethyl ester (122-51-0) → N,N'-di-p-tolylformamidine (16596-03-5,141417-88-1)

Guidance literature:

orthoformic acid triethyl ester; at 20 ℃; for 0.25h;

p-toluidine; at 20 ℃; for 4h;

DOI:10.1016/j.molstruc.2012.06.009

Reference yield: 91.0%

p-toluidine (106-49-0,12221-03-3) + formamide (77287-34-4,77287-35-5,60100-09-6) → N,N'-di-p-tolylformamidine (16596-03-5,141417-88-1)

Guidance literature:

With phosphorus tribromide; at 50 - 60 ℃; Inert atmosphere;

DOI:10.1021/jo301463m

Reference yield: 90.0%

p-toluidine (106-49-0,12221-03-3) + trimethyl orthoformate (149-73-5) → N,N'-di-p-tolylformamidine (16596-03-5,141417-88-1)

Guidance literature:

With 1,1,1,3',3',3'-hexafluoro-propanol; at 20 ℃; for 3h; chemoselective reaction;

DOI:10.1016/j.jfluchem.2010.10.002

upstream raw materials:

methanol

4-methylphenyl isocyanide

isopropyl benzenesulfonate

N-(4-methylphenyl)formamide

Downstream raw materials:

4-hydroxy-6-methyl-quinoline-3-carboxylic acid

2-p-toluidinomethylene-N-p-tolyl-malonamic acid ethyl ester

3,5,6-trichloro-2-(4-methylphenylamino)-1,4-benzoquinone

[Ir((CH₃C₆H₄N)2CH)(C₈H₁₂)]2