3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

Base Information

Chemical Name:3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol
CAS No.:1355330-13-0
Molecular Formula:C₁₈H₁₉N₃O₆
Molecular Weight:373.365
Hs Code.:

Synonyms:3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

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Chemical Property of 3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

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Technology Process of 3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

There total 3 articles about 3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1355330-32-3
1-(4-methoxy-2,3-bis(methoxymethoxy)phenyl)-5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

: 1355330-13-0
3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1016/j.bmc.2011.11.010

Reference yield:

: 290347-62-5
1-bromo-4-methoxy-2,3-bis(methoxymethoxy)-benzene

: 1355330-13-0
3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 15 h / -78 - 20 °C / Inert atmosphere

2.1: ethylmagnesium chloride / tetrahydrofuran / 0.25 h / 50 °C / Inert atmosphere

2.2: 3 h / 50 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran / 5 h / 20 °C

With hydrogenchloride; n-butyllithium; water; ethylmagnesium chloride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2011.11.010

Reference yield:

: 53560-33-1
3,4,5-trimethoxyphenylacetylene

: 1355330-27-6
1-azido-4-methoxy-2,3-bis(methoxymethoxy)benzene

: 1355330-13-0
3-methoxy-6-(5-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazol-1-yl)benzene-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylmagnesium chloride / tetrahydrofuran / 0.25 h / 50 °C / Inert atmosphere

1.2: 3 h / 50 °C / Inert atmosphere

2.1: hydrogenchloride; water / tetrahydrofuran / 5 h / 20 °C

With hydrogenchloride; water; ethylmagnesium chloride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2011.11.010