1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

Base Information

Chemical Name:1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt
CAS No.:872462-76-5
Molecular Formula:C₁₇H₁₈NO₇S*Na
Molecular Weight:403.388
Hs Code.:

Synonyms:1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

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Chemical Property of 1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

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Technology Process of 1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

There total 2 articles about 1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1120-71-4
1,3-propanesultone

: 267875-78-5
3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid ethyl ester

: 872462-76-5
1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

Guidance literature:: 1,3-propanesultone; 3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid ethyl ester; With lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃;

With sodium hydroxide; at 20 ℃; for 6h;

Reference yield: 37.0%

: 1120-71-4
1,3-propanesultone

: 872462-76-5
1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

Guidance literature:: 3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid ethyl ester; With lithium hydroxide; In N,N-dimethyl-formamide;

1,3-propanesultone; In N,N-dimethyl-formamide; at 20 ℃;

With sodium hydroxide; Amberlite IR-120 (H+); more than 3 stages;

Reference yield: 77.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 872462-76-5
1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

: 872462-77-6
1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;