1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

Base Information

• Chemical Name: 1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt
• CAS No.: 872462-77-6
• Molecular Formula: C₂₃H₂₁N₂O₉S*Na
• Molecular Weight: 524.484

Synonyms:1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

Chemical Property of 1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

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Technology Process of 1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

There total 1 articles about 1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt (872462-76-5) → 1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt (872462-77-6)

Guidance literature:

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 82.0%

4-amino-5-[bis(2-aminoethyl)amino]pentanecarboxylic acid (872463-07-5) + 1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt (872462-77-6) → 5-(bis-(2-((1-(3-sulfonatopropyl)-3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl)-amino)-ethyl)-amino)-4-((1-(3-sulfonatopropyl)-3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl)-amino)-pentanoic acid, trisodium salt

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

Reference yield: 82.0%

1-(3-sulfonatopropyl)-4-(4-nitrophenyloxycarbonyl)-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt (872462-77-6) + 4-amino-5-[bis(2-aminoethyl)amino]pentanecarboxylic acid (872462-34-5) → 5-[bis-(2-{[1-(sodium sulfonatopropyl)-3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl]amino}ethyl)amino]-4-{[1-(sodium sulfonatopropyl)-3-benzyloxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl]amino}pentane carboxylic acid

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

upstream raw materials:

4-nitro-phenol

1-(3-sulfonatopropyl)-4-carboxy-3-benzyloxy-6-methyl-1H-pyridin-2-one, sodium salt

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