3-phenylpropyl ethanethiolate

Base Information

• Chemical Name: 3-phenylpropyl ethanethiolate
• CAS No.: 132150-34-6
• Molecular Formula: C₁₁H₁₆S
• Molecular Weight: 180.314
• Mol file: 132150-34-6.mol

Synonyms:3-phenylpropyl ethanethiolate

Chemical Property of 3-phenylpropyl ethanethiolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-phenylpropyl ethanethiolate

There total 5 articles about 3-phenylpropyl ethanethiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3-phenyl-propionaldehyde (104-53-0) + (ethylthio)trimethylsilane (5573-62-6) → 3-phenylpropyl ethanethiolate (132150-34-6)

Guidance literature:

indium(III) chloride; chloro-trimethyl-silane; In dichloromethane; 0 deg C to RT;

DOI:10.1246/bcsj.64.2524

Reference yield: 68.0%

3-phenylpropanal diethyl dithioacetal (128881-93-6) → 3-phenylpropyl ethanethiolate (132150-34-6)

Guidance literature:

3-phenylpropanal diethyl dithioacetal; With digallium tetrachloride; In dichloromethane; at 20 ℃; for 12h;

With sulfuric acid; In dichloromethane; for 0.166667h;

DOI:10.1016/j.tetlet.2005.10.024

Reference yield: 68.0%

1-ethylthio-1-trimethylsiloxy-3-phenylpropane (132150-37-9) → 3-phenylpropyl ethanethiolate (132150-34-6)

Guidance literature:

With triethylsilane; indium(III) chloride; chloro-trimethyl-silane; In dichloromethane; Ambient temperature;

DOI:10.1246/bcsj.64.2524

upstream raw materials:

1-Bromo-3-phenylpropane

sodium thioethylate

3-phenyl-propionaldehyde

(ethylthio)trimethylsilane

Downstream raw materials:

3-Phenylpropane-1-thiol

(S)-(2-nitro-1-phenylethyl)(3-phenylpropyl) sulfide