3-phenylpropanal diethyl dithioacetal

Base Information

• Chemical Name: 3-phenylpropanal diethyl dithioacetal
• CAS No.: 128881-93-6
• Molecular Formula: C₁₃H₂₀S₂
• Molecular Weight: 240.434

Synonyms:3-phenylpropanal diethyl dithioacetal

Chemical Property of 3-phenylpropanal diethyl dithioacetal

Chemical Property:

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Technology Process of 3-phenylpropanal diethyl dithioacetal

There total 1 articles about 3-phenylpropanal diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-phenyl-propionaldehyde (104-53-0) + ethanethiol (75-08-1) → 3-phenylpropanal diethyl dithioacetal (128881-93-6)

Guidance literature:

With tantalum pentachloride; In dichloromethane; for 0.0833333h; Ambient temperature;

DOI:10.1016/S0040-4020(97)01051-X

Reference yield: 84.0%

allyltributylstanane (24850-33-7) + 3-phenylpropanal diethyl dithioacetal (128881-93-6) → (3-Ethylsulfanyl-hex-5-enyl)-benzene (130839-76-8)

Guidance literature:

With gallium(III) trichloride; In dichloromethane; at -23 ℃; for 30h;

DOI:10.1246/cl.1990.1097

Reference yield: 77.0%

crotyltributylstannane (31197-41-8,76505-19-6) + 3-phenylpropanal diethyl dithioacetal (128881-93-6) → (3-Ethylsulfanyl-4-methyl-hex-5-enyl)-benzene (615538-25-5)

Guidance literature:

With gallium(III) trichloride; In dichloromethane; at -23 ℃; for 30h;

DOI:10.1246/cl.1990.1097

upstream raw materials:

3-phenyl-propionaldehyde

ethanethiol

Downstream raw materials:

(3-Ethylsulfanyl-hex-5-enyl)-benzene

(3-Ethylsulfanyl-5-methyl-hex-5-enyl)-benzene

(3-Ethylsulfanyl-4-methyl-hex-5-enyl)-benzene

3-phenyl-propionaldehyde

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