2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Base Information

• Chemical Name: 2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate
• CAS No.: 330556-10-0
• Molecular Formula: C₂₅H₃₄F₄O₄S
• Molecular Weight: 506.602

Synonyms:2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Chemical Property of 2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Chemical Property:

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Technology Process of 2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

There total 2 articles about 2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

Farnesol (106-28-5) + 2-Methylpropan-1-yl pentafluorobenzenesulfonate (330556-05-3) → 2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate (330556-10-0)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/b007101n

Reference yield:

pentafluorobenzenesulonyl chloride (832-53-1) → 2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate (330556-10-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 64 percent / pyridine / diethyl ether / 17 h / 20 °C

2: 60 percent / aq. NaOH; Bu₄N(+)HSO₄(-) / CH₂Cl₂ / 1 h / 20 °C

With pyridine; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; dichloromethane;

DOI:10.1039/b007101n

Reference yield: 50.0%

2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate (330556-10-0) → 2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate (330556-06-4)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In toluene; at 0 - 20 ℃; for 1h;

DOI:10.1039/b007101n

upstream raw materials:

Farnesol

2-Methylpropan-1-yl pentafluorobenzenesulfonate

pentafluorobenzenesulonyl chloride

Downstream raw materials:

2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

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