2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Base Information

Chemical Name:2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate
CAS No.:330556-06-4
Molecular Formula:C₂₅H₃₅F₃O₅S
Molecular Weight:504.611
Hs Code.:

Synonyms:2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

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Chemical Property of 2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

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Technology Process of 2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

There total 4 articles about 2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 330556-10-0
2-Methylpropan-1-yl 2,3,4,5-tetrafluoro-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

: 330556-06-4
2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In toluene; at 0 - 20 ℃; for 1h;
DOI:10.1039/b007101n

Reference yield:

: 106-28-5
Farnesol

: 330556-06-4
2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / aq. NaOH; Bu₄N(+)HSO₄(-) / CH₂Cl₂ / 1 h / 20 °C

2: 50 percent / aq. NaOH; Bu₄N(+)HSO₄(-) / toluene / 1 h / 0 - 20 °C

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; toluene;
DOI:10.1039/b007101n

Reference yield:

: 832-53-1
pentafluorobenzenesulonyl chloride

: 330556-06-4
2-Methylpropan-1-yl 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / pyridine / diethyl ether / 17 h / 20 °C

2: 60 percent / aq. NaOH; Bu₄N(+)HSO₄(-) / CH₂Cl₂ / 1 h / 20 °C

3: 50 percent / aq. NaOH; Bu₄N(+)HSO₄(-) / toluene / 1 h / 0 - 20 °C

With pyridine; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; dichloromethane; toluene;
DOI:10.1039/b007101n