C₈₁H₉₉F₁₃NO₂₄P₃

Base Information

• Chemical Name: C₈₁H₉₉F₁₃NO₂₄P₃
• CAS No.: 1571060-63-3
• Molecular Formula: C₈₁H₉₉F₁₃NO₂₄P₃
• Molecular Weight: 1810.57
• Mol file: 1571060-63-3.mol

Synonyms:C₈₁H₉₉F₁₃NO₂₄P₃

Chemical Property of C₈₁H₉₉F₁₃NO₂₄P₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₈₁H₉₉F₁₃NO₂₄P₃

There total 1 articles about C₈₁H₉₉F₁₃NO₂₄P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

C34H44F13NO7 (1571060-62-2) + benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite (108549-21-9) + 1D-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzyl phosphate) (496808-69-6) → C81H99F13NO24P3 (1571060-63-3)

Guidance literature:

C₃₄H₄₄F₁₃NO₇; benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

1D-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzyl phosphate); With 1H-tetrazole; In dichloromethane; at 20 ℃; Inert atmosphere;

With tert.-butylhydroperoxide; In dichloromethane; at -40 - 20 ℃; Inert atmosphere;

DOI:10.1039/c4cc00022f

Reference yield:

C81H99F13NO24P3 (1571060-63-3) → C38H63F13NO22P3

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; for 6h;

DOI:10.1039/c4cc00022f

upstream raw materials:

C₃₄H₄₄F₁₃NO₇

benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

1D-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzyl phosphate)