(R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

Base Information

Chemical Name:(R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one
CAS No.:1613271-12-7
Molecular Formula:C₂₉H₄₈O₄Si₂
Molecular Weight:516.869
Hs Code.:

Synonyms:(R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

Suppliers and Price of (R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

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Chemical Property of (R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

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Technology Process of (R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

There total 11 articles about (R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (6R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-ol

: 1613271-12-7
(R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 16h; Inert atmosphere;

Reference yield:

: 94956-98-6
2-allyl-3-methoxybenzaldehyde

: 1613271-12-7
(R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sec.-butyllithium / tert-butyl methyl ether; cyclohexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 17 h / -78 - 20 °C

2.1: manganese(IV) oxide / dichloromethane / 16 h / Inert atmosphere

With manganese(IV) oxide; sec.-butyllithium; In dichloromethane; tert-butyl methyl ether; cyclohexane;

Reference yield:

: 1613271-09-2
(R)-5-(but-3-yn-1-yl)-2,2,3,3,8,8,9,9-octamethyl-4,7-dioxa-3,8-disiladecane

: 1613271-12-7
(R)-1-(2-allyl-3-methoxyphenyl)-6,7-bis((tert-butyldimethylsilyl)oxy)hept-2-yn-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sec.-butyllithium / tert-butyl methyl ether; cyclohexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 17 h / -78 - 20 °C

2.1: manganese(IV) oxide / dichloromethane / 16 h / Inert atmosphere

With manganese(IV) oxide; sec.-butyllithium; In dichloromethane; tert-butyl methyl ether; cyclohexane;