5-Phenyl-2-thiaadamantane

Base Information

Chemical Name:5-Phenyl-2-thiaadamantane
CAS No.:153171-89-2
Molecular Formula:C₁₅H₁₈S
Molecular Weight:230.374
Hs Code.:

Synonyms:5-Phenyl-2-thiaadamantane

Suppliers and Price of 5-Phenyl-2-thiaadamantane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Phenyl-2-thiaadamantane

Chemical Property:

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Technology Process of 5-Phenyl-2-thiaadamantane

There total 5 articles about 5-Phenyl-2-thiaadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1-Phenyl-3,7-exo,exo-diiodobicyclo<3.3.1>nonane

: 153171-89-2
5-Phenyl-2-thiaadamantane

Guidance literature:: With sodium sulfide; In ethanol; for 10h; Heating;
DOI:10.1021/jo00079a056

Reference yield:

: 38584-33-7
5-phenyladamantan-2-one

: 153171-89-2
5-Phenyl-2-thiaadamantane

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / m-CPBA / CH₂Cl₂ / Ambient temperature

2: 85 percent / tetrahydrofuran / 0.25 h / -78 °C

3: 85 percent / pyridine, yellow HgO, I₂ / benzene / 1.) r.t., 2.) irradiation, 2 h

4: 75 percent / iodotrimethylsilane / CCl₄ / 72 h / Ambient temperature

5: 65 percent / Na₂S*9H₂O / ethanol / 10 h / Heating

With pyridine; sodium sulfide; trimethylsilyl iodide; iodine; 3-chloro-benzenecarboperoxoic acid; mercury(II) oxide; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; benzene;
DOI:10.1021/jo00079a056

Reference yield:

: 153171-91-6
1-Phenyl-4-oxatricyclo<4.4.1.1^3,8>undecan-5-one

: 153171-89-2
5-Phenyl-2-thiaadamantane

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / tetrahydrofuran / 0.25 h / -78 °C

2: 85 percent / pyridine, yellow HgO, I₂ / benzene / 1.) r.t., 2.) irradiation, 2 h

3: 75 percent / iodotrimethylsilane / CCl₄ / 72 h / Ambient temperature

4: 65 percent / Na₂S*9H₂O / ethanol / 10 h / Heating

With pyridine; sodium sulfide; trimethylsilyl iodide; iodine; mercury(II) oxide; In tetrahydrofuran; tetrachloromethane; ethanol; benzene;
DOI:10.1021/jo00079a056