1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

Base Information

Chemical Name:1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone
CAS No.:870258-69-8
Molecular Formula:C₂₄H₂₈N₂O₄
Molecular Weight:408.497
Hs Code.:

Synonyms:1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

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Chemical Property of 1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

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Technology Process of 1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

There total 4 articles about 1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108-24-7
acetic anhydride

: 133603-96-0
C₂₀H₂₄N₂O₂

: 870258-69-8
1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 24h;
DOI:10.1002/adsc.200606013

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 870258-69-8
1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 12 h / Heating

2: 52.3 g / Mn powder; CF₃COOH / acetonitrile; toluene / 24 h / 20 °C

3: 91 percent / K₂CO₃ / dimethylformamide / 24 h / 120 °C

With manganese; potassium carbonate; trifluoroacetic acid; In ethanol; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/adsc.200606013

Reference yield:

: 3187-83-5,41013-27-8,41013-28-9,64346-55-0,150026-23-6,133695-16-6,176776-60-6
(R,R)-N,N'-bis(salicylidene)-1,2-cyclohexanediamine

: 870258-69-8
1-[(2S,3S,4aR,8aR)-4-Acetyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 52.3 g / Mn powder; CF₃COOH / acetonitrile; toluene / 24 h / 20 °C

2: 91 percent / K₂CO₃ / dimethylformamide / 24 h / 120 °C

With manganese; potassium carbonate; trifluoroacetic acid; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/adsc.200606013