dimethyl undecylphosphonate

Base Information

• Chemical Name: dimethyl undecylphosphonate
• CAS No.: 76964-70-0
• Molecular Formula: C₁₃H₂₉O₃P
• Molecular Weight: 264.345
• Mol file: 76964-70-0.mol

Synonyms:dimethyl undecylphosphonate

Chemical Property of dimethyl undecylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethyl undecylphosphonate

There total 1 articles about dimethyl undecylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl phosphite (96-36-6,868-85-9) + 1-undecene (821-95-4) → dimethyl undecylphosphonate (76964-70-0)

Guidance literature:

Irradiation_.UV-Licht;

Reference yield:

dimethyl undecylphosphonate (76964-70-0) → (+)-O-hexyl O-(p-nitrophenyl) n-undecylphosphonate

Guidance literature:

Multi-step reaction with 3 steps

1.1: 95 percent / oxalyl chloride / diethyl ether / 72 h / Heating

2.1: N-methylimidazole / CH₂Cl₂

3.1: N-methylimidazole / CH₂Cl₂ / 0.25 h

3.2: Daicel Chiralpack AS column

With 1-methyl-1H-imidazole; oxalyl dichloride; In diethyl ether; dichloromethane; 1.1: Chlorination / 2.1: Substitution / 3.1: Substitution / 3.2: Racemate resolution;

DOI:10.1016/S0009-3084(99)00028-6

Reference yield:

dimethyl undecylphosphonate (76964-70-0) → O-methyl O-(p-nitrophenyl) n-undecylphosphonate

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / oxalyl chloride / diethyl ether / 72 h / Heating

2: N-methylimidazole / CH₂Cl₂

3: 53 percent / N-methylimidazole / CH₂Cl₂ / 0.25 h

With 1-methyl-1H-imidazole; oxalyl dichloride; In diethyl ether; dichloromethane; 1: Chlorination / 2: Substitution / 3: Substitution;

DOI:10.1016/S0009-3084(99)00028-6

upstream raw materials:

methyl phosphite

1-undecene

Downstream raw materials:

undecyl-phosphonic acid