tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

Base Information

Chemical Name:tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate
CAS No.:1416332-50-7
Molecular Formula:C₁₉H₂₄N₂O₄
Molecular Weight:344.411
Hs Code.:

Synonyms:tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

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Chemical Property of tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

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Technology Process of tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

There total 6 articles about tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.9%

: 1416332-43-8
(E)-tert-butyl (2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)carbamate

: 49639-34-1,90617-28-0
phenylsulfinylacetic acid amide

: 1416332-50-7
tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

Guidance literature:: (E)-tert-butyl (2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)carbamate; phenylsulfinylacetic acid amide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 50 ℃; for 4h; Inert atmosphere;

With acetic acid; In acetonitrile; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/ol500162b

Reference yield:

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 1416332-50-7
tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; diethylazodicarboxylate / benzene; toluene / 0 - 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 4 h / 50 °C / Inert atmosphere

3: acetic acid / acetonitrile / Inert atmosphere; Reflux

4: acetic acid / acetonitrile / Inert atmosphere; Reflux

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; lithium chloride; diethylazodicarboxylate; In toluene; acetonitrile; benzene;
DOI:10.1021/ol303320c

Reference yield:

: 1416332-43-8
(E)-tert-butyl (2-(3-(3-oxobut-1-en-1-yl)phenoxy)ethyl)carbamate

: 1416332-50-7
tert-butyl (2-(3-(6-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenoxy)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 4 h / 50 °C / Inert atmosphere

2: acetic acid / acetonitrile / Inert atmosphere; Reflux

3: acetic acid / acetonitrile / Inert atmosphere; Reflux

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile;
DOI:10.1021/ol303320c