Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI)

Base Information

Chemical Name:Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI)
CAS No.:177266-29-4
Molecular Formula:C₁₀H₁₂O
Molecular Weight:148.205
Hs Code.:
Mol file:177266-29-4.mol

Synonyms:Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI)

Suppliers and Price of Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI)

Chemical Property:

PSA：17.07000
LogP:1.95370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI)

There total 6 articles about Ethanone, 1-(3-methylenebicyclo[2.2.1]hept-5-en-2-yl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2200-53-5
penta-3,4-dien-2-one

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 59435-86-8,84653-64-5,177266-29-4
endo-2-Acetyl-3-methylenebicyclo<2.2.1>hept-5-ene

Guidance literature:: With zinc(II) chloride; In dichloromethane;

Reference yield: 60.0%

: endo-2-(1-Hydroxyethyl)-3-methylenebicyclo<2.2.1>hept-5-ene

: 59435-86-8,84653-64-5,177266-29-4
endo-2-Acetyl-3-methylenebicyclo<2.2.1>hept-5-ene

Guidance literature:: With pyridine; chromium(VI) oxide; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo00084a019

Reference yield:

: 82431-31-0
endo(1S*,2R*,4R*)-3-methylenebicyclo[2.2.1]hept-5-enyl-2-carbaldehyde

: 59435-86-8,84653-64-5,177266-29-4
endo-2-Acetyl-3-methylenebicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / diethyl ether / 6 h / Heating

2: 60 percent / CrO₃, pyridine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; chromium(VI) oxide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00084a019