1,8-bisiodo>-1,7-octadiyne

Base Information

• Chemical Name: 1,8-bisiodo>-1,7-octadiyne
• CAS No.: 138877-43-7
• Molecular Formula: 2CF₃O₃S*C₂₀H₁₈I₂
• Molecular Weight: 810.313

Synonyms:1,8-bisiodo>-1,7-octadiyne

Chemical Property of 1,8-bisiodo>-1,7-octadiyne

Chemical Property:

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Technology Process of 1,8-bisiodo>-1,7-octadiyne

There total 1 articles about 1,8-bisiodo>-1,7-octadiyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

oxy>iodo>benzene (129540-75-6) + 1,8-bis(tributylstannyl)-1,7-octadiyne (138877-33-5) → 1,8-bisiodo>-1,7-octadiyne (138877-43-7)

Guidance literature:

In dichloromethane; at -78 - 0 ℃; for 0.166667h;

DOI:10.1021/jo00032a046

Reference yield: 67.0%

1,8-bisiodo>-1,7-octadiyne (138877-43-7) + triphenylphosphine (603-35-0) → iodobenzene (591-50-4) + 1,8-bisphosphoranyl>-1,7-octadiyne (138877-55-1)

Guidance literature:

In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1021/jo00032a046

upstream raw materials:

oxy>iodo>benzene

1,8-bis(tributylstannyl)-1,7-octadiyne

Downstream raw materials:

iodobenzene

1,8-bisphosphoranyl>-1,7-octadiyne

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