6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Base Information

Chemical Name:6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine
CAS No.:1383948-59-1
Molecular Formula:C₂₂H₂₁N₃OS
Molecular Weight:375.494
Hs Code.:

Synonyms:6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

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Chemical Property of 6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

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Technology Process of 6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

There total 3 articles about 6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383944-56-6
6-bromo-2-(2-ethyl-sulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

: 100-51-6,185532-71-2
benzyl alcohol

: 1383948-59-1
6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In 1-methyl-pyrrolidin-2-one; xylene; at 150 ℃; for 8h; Cooling with ice;

Reference yield:

: 89415-54-3
5-bromo-N²-methylpyridine-2,3-diamine

: 1383948-59-1
6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 0.5 h / 120 °C

1.2: 1 h / 140 °C

2.1: caesium carbonate; 1,10-Phenanthroline; copper(l) iodide / 1-methyl-pyrrolidin-2-one; xylene / 8 h / 150 °C / Cooling with ice

With copper(l) iodide; 1,10-Phenanthroline; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1-methyl-pyrrolidin-2-one; xylene;

Reference yield:

: 21101-79-1
2-ethylsulfanylbenzoic acid

: 1383948-59-1
6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 0.5 h / 120 °C

1.2: 1 h / 140 °C

2.1: caesium carbonate; 1,10-Phenanthroline; copper(l) iodide / 1-methyl-pyrrolidin-2-one; xylene / 8 h / 150 °C / Cooling with ice

With copper(l) iodide; 1,10-Phenanthroline; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1-methyl-pyrrolidin-2-one; xylene;