S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

Base Information

Chemical Name:S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate
CAS No.:1383948-60-4
Molecular Formula:C₁₇H₁₇N₃O₃S₃
Molecular Weight:407.538
Hs Code.:

Synonyms:S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

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Chemical Property of S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

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Technology Process of S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

There total 6 articles about S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 1383946-82-4
2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-ol

: 74-88-4
methyl iodide

: 1383948-60-4
S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

Guidance literature:: 2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-ol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 50 ℃; for 1h; Cooling with ice;

carbon disulfide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 2.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; for 1.5h;

Reference yield:

: 1383948-59-1
6-benzyloxy-2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

: 1383948-60-4
S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane; chloroform / 3 h / Cooling with ice

2.1: 3-chloro-benzenecarboperoxoic acid / chloroform; acetonitrile / 3 h / Cooling with ice

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 50 °C / Cooling with ice

3.2: 2.5 h / 20 °C

3.3: 1.5 h

With boron tribromide; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1383946-81-3
2-(2-ethylsulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-ol

: 1383948-60-4
S-methyl O-[2-(2-ethylsulfonyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine-6-yl] dithiocarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / chloroform; acetonitrile / 3 h / Cooling with ice

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 50 °C / Cooling with ice

2.2: 2.5 h / 20 °C

2.3: 1.5 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In chloroform; N,N-dimethyl-formamide; acetonitrile; mineral oil;