N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide
CAS No.:1591958-14-3
Molecular Formula:C₁₈H₂₀N₂O₃S
Molecular Weight:344.434
Hs Code.:

Synonyms:N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

Suppliers and Price of N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

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Technology Process of N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

There total 5 articles about N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 941-55-9
4-toluenesulfonyl azide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 536-74-3
phenylacetylene

: 1591958-14-3
N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

Guidance literature:: phenylacetylene; With copper(I) thiophene-2-carboxylate; benzoic acid; In water; benzene; for 0.5h; Sonication;

4-toluenesulfonyl azide; In water; benzene; Flow reactor;

N,N-dimethyl-formamide; With rhodium(II) pivalate; In benzene; for 1.33333h; Flow reactor;

Reference yield: 84.0%

: 884866-01-7
1-(4-methylbenzensulfonyl)-4-phenyl-1H-1,2,3-triazole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1591958-14-3
N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

Guidance literature:: With rhodium(II) pivalate; In chloroform; at 60 ℃; for 1h; regioselective reaction; Molecular sieve;
DOI:10.1021/ol5010774

Reference yield: 79.0%

: 884866-01-7
1-(4-methylbenzensulfonyl)-4-phenyl-1H-1,2,3-triazole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1591958-14-3
N-[(1Z)-1-(dimethylamino)-3-oxo-3-phenylprop-1-en-2-yl]-4-methylbenzenesulfonamide

: 93961-59-2
2-(dimethylamino)-5-phenyl-1,3-oxazole

Guidance literature:: With rhodium(II) pivalate; In chloroform; at 120 ℃; for 0.25h; regioselective reaction; Molecular sieve;
DOI:10.1021/ol5010774