(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

Base Information

Chemical Name:(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol
CAS No.:190388-66-0
Molecular Formula:C₁₄H₂₆O₂
Molecular Weight:226.359
Hs Code.:

Synonyms:(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

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Technology Process of (-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

There total 9 articles about (-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 190388-82-0
methyl (1R,2R,4aS,8aS)-2-hydroxydecahydro-5,5,8a-trimethylnaphthalene-1-carboxylate

: 190388-66-0,807360-95-8
(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1248/cpb.45.824

Reference yield: 96.0%

: Acetic acid 8-((3S,4aR,6aS,10aS,10bS)-7,7,10a-trimethyl-decahydro-naphtho[2,1-d][1,3]dioxin-3-yl)-naphthalen-1-yl ester

: 190388-66-0,807360-95-8
(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

Guidance literature:: With hydrogen; palladium hydroxide - carbon; In methanol; Ambient temperature;
DOI:10.1016/S0957-4166(98)00172-4

Reference yield:

: 59633-91-9,65754-93-0,108944-87-2,108944-88-3,136982-34-8,146611-16-7,807360-95-8
rac-12-nor-drimane-8α,11-diol

: 190388-66-0,807360-95-8
(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / conc. H₂SO₄ / dimethylsulfoxide / 1 h / Ambient temperature

2: 99 percent / p-dimethylaminopyridine, pyridine / 1 h / Ambient temperature

4: 96 percent / H₂ / 20percent Pd(OH)2-C / methanol / Ambient temperature

With pyridine; dmap; sulfuric acid; hydrogen; palladium hydroxide - carbon; In methanol; dimethyl sulfoxide;
DOI:10.1016/S0957-4166(98)00172-4