(isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

Base Information

Chemical Name:(isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride
CAS No.:1388842-23-6
Molecular Formula:C₁₈H₁₈F₃N₃O₆S
Molecular Weight:461.419
Hs Code.:

Synonyms:(isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

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Chemical Property of (isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

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Technology Process of (isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

There total 6 articles about (isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388842-21-4
(Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic acid

: 543-27-1
isobutyl chloroformate

: 1388842-23-6
(isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

Reference yield:

: 1333153-95-9
3-(methylthio)-5-(trifluoromethyl)benzamide

: 1388842-23-6
(isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

Guidance literature:: Multi-step reaction with 7 steps

1.1: Oxone / acetone / 12 h / 20 °C

2.1: thionyl chloride / N,N-dimethyl-formamide / 12 h / 90 °C

3.1: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C

4.1: hydrazine hydrate / N,N-dimethyl-formamide / 3 h

4.2: 90 °C

5.1: triethylamine / dichloromethane / 0 °C

6.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

6.2: Acidic conditions

7.1: 4-methyl-morpholine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; sodium hydrogen sulfide; Oxone; thionyl chloride; water; hydrazine hydrate; triethylamine; magnesium chloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1333153-96-0
3-(methylsulfonyl)-5-(trifluoromethyl)benzamide

: 1388842-23-6
(isobutyl carbonic) (Z)-3-(3-(3-(methylsulfonyl)-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazol-1-yl)acrylic anhydride

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / 12 h / 90 °C

2.1: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C

3.1: hydrazine hydrate / N,N-dimethyl-formamide / 3 h

3.2: 90 °C

4.1: triethylamine / dichloromethane / 0 °C

5.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

5.2: Acidic conditions

6.1: 4-methyl-morpholine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; sodium hydrogen sulfide; thionyl chloride; water; hydrazine hydrate; triethylamine; magnesium chloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;