allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Base Information

Chemical Name:allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside
CAS No.:1392224-77-9
Molecular Formula:C₇₁H₈₆Cl₃NO₂₀Si
Molecular Weight:1407.9
Hs Code.:

allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Synonyms:allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

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Chemical Property of allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

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Technology Process of allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

There total 1 articles about allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1250346-64-5
allyl 4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1-4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: 612844-13-0
Acetic acid (4aR,6S,7R,8R,8aR)-2,2-di-tert-butyl-6-phenylsulfanyl-7-(2,2,2-trichloro-ethoxycarbonylamino)-hexahydro-1,3,5-trioxa-2-sila-naphthalen-8-yl ester

: 1392224-77-9
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja306274v

Reference yield: 80.0%

: 1392224-77-9
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: C₆₈H₈₂Cl₃NO₂₀Si

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja306274v

Reference yield: 72.0%

: 1392224-77-9
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: 1392224-78-0
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja306274v