allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Base Information

Chemical Name:allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside
CAS No.:1392224-78-0
Molecular Formula:C₆₀H₇₈Cl₃NO₂₀Si
Molecular Weight:1267.72
Hs Code.:

allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Synonyms:allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

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Chemical Property of allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

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Technology Process of allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

There total 1 articles about allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1392224-77-9
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: 1392224-78-0
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja306274v

Reference yield: 72.0%

: 1392224-78-0
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: 1371597-38-4
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl N-phenyltrifluoroacetimidate

: 1392224-80-4
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-[2,3,4,6-tetra-O-benzyl-α-D-glycopyranosyl]-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trifluorormethanesulfonic acid; In diethyl ether; at -30 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja306274v

Reference yield: 10.0%

: 3,4,6-tri-O-acetyl-2-O-[(S)-2-(phenylthiomethyl)benzyl]-D-glucopyranosyl trifluoro-[N-phenyl]-acetimidate

: 1392224-78-0
allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: 1392224-79-1
C₈₆H₁₀₆Cl₃NO₂₈SSi

Guidance literature:: 3,4,6-tri-O-acetyl-2-O-[(S)-2-(phenylthiomethyl)benzyl]-D-glucopyranosyl trifluoro-[N-phenyl]-acetimidate; With trifluorormethanesulfonic acid; In dichloromethane; at -35 - 0 ℃; for 0.5h; Inert atmosphere;

allyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tertbutylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at -35 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja306274v