N²-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine

Base Information

• Chemical Name: N²-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine
• CAS No.: 652160-07-1
• Molecular Formula: C₇₂H₆₈N₆O₆
• Molecular Weight: 1113.37

Synonyms:N²-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine

Chemical Property of N²-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine

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Technology Process of N²-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine

There total 1 articles about N²-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

mono-4-methoxytrityl chloride (14470-28-1) + 8-dimethylamino-9-[4-hydroxy-3-(hydroxymethyl)butyl]guanine (652160-06-0) → N2-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine (652160-07-1)

Guidance literature:

With dmap; triethylamine; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 3h;

DOI:10.1055/s-2003-42454

Reference yield: 98.0%

methyl trifluoromethanesulfonate (333-27-7) + N2-(p-anisyldiphenylmethyl)-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine (652160-07-1) → N2-(p-anisyldiphenylmethyl)-7-methyl-8-dimethylamino-9-[(4-p-anisyldiphenylmethoxy)-3-p-anisyldiphenylmethoxymethylbutyl]guanine-8-triflate

Guidance literature:

In dichloromethane;

DOI:10.1055/s-2003-42454

upstream raw materials:

mono-4-methoxytrityl chloride

8-dimethylamino-9-[4-hydroxy-3-(hydroxymethyl)butyl]guanine

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