1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

Base Information

Chemical Name:1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle
CAS No.:143739-66-6
Molecular Formula:C₂₉H₃₁N₃O₅
Molecular Weight:501.582
Hs Code.:

Synonyms:1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

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Chemical Property of 1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

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Technology Process of 1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

There total 5 articles about 1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 143739-64-4
1,2-dihydro-6,7-dimethoxy-N-methylisoquinoleine-3-carboxylate d'ethyle

: 40277-63-2
4-methoxy-N'-phenylbenzohydrazonoyl chloride

: 143739-66-6
1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

Guidance literature:: With triethylamine; In benzene; for 24h; Heating;

Reference yield:

: 136413-54-2
6,7-dimethoxy-3,4-dihydroisoquinoleine-3,3-dicarboxylate de diethyle

: 143739-66-6
1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

Guidance literature:: Multi-step reaction with 5 steps

1: 2) ethanol, H(+)

2: air / ethanol / 0.25 h / Heating

3: 76 percent / acetone / 12 h / Ambient temperature

4: 92 percent / NaBH₄ / ethanol; H₂O / 4 h

5: 53 percent / triethylamine / benzene / 24 h / Heating

With sodium tetrahydroborate; air; ethanol; hydrogen cation; triethylamine; In ethanol; water; acetone; benzene;

Reference yield:

: 143739-60-0
3,4-dihydro-6,7-dimethoxyquinoleine-3-carboxylate d'ethyle

: 143739-66-6
1-para-anisyl-7,8-dimethoxy-4-methyl-3-phenyl-3a,4,5,9b-tetrahydropyrazolo<3,4-c>isoquinoleine-3a-carboxylate d'ethyle

Guidance literature:: Multi-step reaction with 4 steps

1: air / ethanol / 0.25 h / Heating

2: 76 percent / acetone / 12 h / Ambient temperature

3: 92 percent / NaBH₄ / ethanol; H₂O / 4 h

4: 53 percent / triethylamine / benzene / 24 h / Heating

With sodium tetrahydroborate; air; triethylamine; In ethanol; water; acetone; benzene;