2,4-dinitrophenyl piperidine-1-carbodithioate

Base Information

• Chemical Name: 2,4-dinitrophenyl piperidine-1-carbodithioate
• CAS No.: 897-73-4
• Molecular Formula: C₁₂H₁₃N₃O₄S₂
• Molecular Weight: 327.385
• Mol file: 897-73-4.mol

Synonyms:Benzenethiol,2,4-dinitro-, 1-piperidinecarbodithioate (ester);2,4-Dinitrophenyl-1-piperidine carbodithioate; NSC 310250

Chemical Property of 2,4-dinitrophenyl piperidine-1-carbodithioate

Chemical Property:

• Vapor Pressure: 2.9E-09mmHg at 25°C
• Boiling Point: 477°Cat760mmHg
• Flash Point: 242.3°C
• Density: 1.49g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-dinitrophenyl piperidine-1-carbodithioate

There total 3 articles about 2,4-dinitrophenyl piperidine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + triethylammonium piperidinodithiocarbamate (59983-55-0) → Piperidino-dithiocarbamidsaeure-(2,4-dinitrophenylester) (897-73-4)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1021/jm3006004

Reference yield:

piperidine (110-89-4) → Piperidino-dithiocarbamidsaeure-(2,4-dinitrophenylester) (897-73-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 20 °C

2: N,N-dimethyl-formamide / 12 h / 20 °C

In N,N-dimethyl-formamide; 2: Sanger reaction;

DOI:10.1021/jm3006004

Reference yield:

→ Piperidino-dithiocarbamidsaeure-(2,4-dinitrophenylester) (897-73-4)

Guidance literature:

Aus Pyridin-N-dithiocarbonsaeure-salz in H2O u. 2,4-Dinitrochlorbenzol in Ethanol;

upstream raw materials:

piperidine

2,4-Dinitrofluorobenzene

triethylammonium piperidinodithiocarbamate

Refernces