(3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

Base Information

Chemical Name:(3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene
CAS No.:176237-30-2
Molecular Formula:C₂₀H₂₅NO₅
Molecular Weight:359.422
Hs Code.:

Synonyms:(3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

Suppliers and Price of (3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

Chemical Property:

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Technology Process of (3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

There total 5 articles about (3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 176484-09-6
(3S,4R,5S)-3-benzoylamino-4,5-isopropylidenedioxycyclopent-1-ene

: 176237-30-2
(3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1055/s-1996-4197

Reference yield:

: 98-88-4
benzoyl chloride

: 176237-30-2
(3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃ / diethyl ether; H₂O / 0.5 h / Ambient temperature

2: 80 percent / diphenyl ether / 1.25 h / Heating

3: 99 percent / Et₃N, 4-N,N-dimethylaminopyridine / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; In diphenylether; diethyl ether; dichloromethane; water;
DOI:10.1055/s-1996-4197

Reference yield:

: C₁₃H₁₉NO₂

: 176237-30-2
(3S,4R,5S)-benzoyl(tert-butylcarbonyl)amino-4,5-isopropylidenedioxycyclopent-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃ / diethyl ether; H₂O / 0.5 h / Ambient temperature

2: 80 percent / diphenyl ether / 1.25 h / Heating

3: 99 percent / Et₃N, 4-N,N-dimethylaminopyridine / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; In diphenylether; diethyl ether; dichloromethane; water;
DOI:10.1055/s-1996-4197