6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Base Information

Chemical Name:6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride
CAS No.:23428-49-1
Molecular Formula:C₃₇H₃₃NO₃*ClH
Molecular Weight:576.135
Hs Code.:

Synonyms:6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

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Chemical Property of 6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Chemical Property:

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Technology Process of 6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

There total 6 articles about 6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23428-48-0
N-(3,4-dibenzyloxyphenethyl)-4-benzyloxyphenylacetamide

6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride: 23428-49-1
6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Guidance literature:: With trichlorophosphate; In acetonitrile; for 0.416667h; Heating;
DOI:10.1039/P19810002016

Reference yield:

: 838-96-0
2-[4-(benzyloxy)phenyl]acetonitrile

6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride: 23428-49-1
6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide, water / ethane-1,2-diol / 18 h / Heating

2: oxalyl chloride, DMF / benzene / 1 h / 20 °C

3: sodium hydrogen carbonate / CH₂Cl₂; H₂O / 1.5 h

4: phosphorus oxychloride / acetonitrile / 0.42 h / Heating

With potassium hydroxide; oxalyl dichloride; water; sodium hydrogencarbonate; N,N-dimethyl-formamide; trichlorophosphate; In dichloromethane; water; ethylene glycol; acetonitrile; benzene;
DOI:10.1039/P19810002016

Reference yield:

: 39188-62-0
2-(4-(benzyloxy)phenyl)acetyl chloride

6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride: 23428-49-1
6,7-bisbenzyloxy-1-(4-benzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogen carbonate / CH₂Cl₂; H₂O / 1.5 h

2: phosphorus oxychloride / acetonitrile / 0.42 h / Heating

With sodium hydrogencarbonate; trichlorophosphate; In dichloromethane; water; acetonitrile;
DOI:10.1039/P19810002016