({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide

Base Information

Chemical Name:({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide
CAS No.:267669-10-3
Molecular Formula:C₁₆H₂₃NO₃Si
Molecular Weight:305.449
Hs Code.:

Synonyms:({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide

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Chemical Property of ({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide

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Technology Process of ({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide

There total 8 articles about ({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 267668-95-1
4,5-dimethoxy-2-[3'-(trimethylsilyl)prop-2'-ynyl]benzaldehyde

: 267669-10-3
({4',5'-dimethoxy-2'-[3-(trimethylsilyl)prop-2-ynyl]phenyl}methylene)methylamine N-oxide

Guidance literature:: With sodium acetate; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1002/1099-0690(200109)2001:17<3313::AID-EJOC3313>3.0.CO;2-E

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 267669-10-3
C₁₆H₂₃NO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: PTSA

2.1: n-BuLi

2.2: MgBr₂

3.1: aq. PTSA / acetone

4.1: NaOAc / CH₂Cl₂

With n-butyllithium; sodium acetate; toluene-4-sulfonic acid; In dichloromethane; acetone; 1.1: Condensation / 2.1: Substitution / 2.2: Grignard reaction / 2.3: Substitution / 3.1: Hydrolysis / 4.1: Condensation;
DOI:10.1021/ol0056832

Reference yield:

: 103477-58-3
2-(2-bromo-4,5-dimethoxyphenyl)-1,3-dioxolane

: 267669-10-3
C₁₆H₂₃NO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi

1.2: MgBr₂

2.1: aq. PTSA / acetone

3.1: NaOAc / CH₂Cl₂

With n-butyllithium; sodium acetate; toluene-4-sulfonic acid; In dichloromethane; acetone; 1.1: Substitution / 1.2: Grignard reaction / 1.3: Substitution / 2.1: Hydrolysis / 3.1: Condensation;
DOI:10.1021/ol0056832