O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol

Base Information

• Chemical Name: O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol
• CAS No.: 107035-78-9
• Molecular Formula: C₄₉H₆₅N₅O₁₆S₇
• Molecular Weight: 1204.54

Synonyms:O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol

Chemical Property of O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol

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Technology Process of O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol

There total 2 articles about O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methanesulfonyl chloride (124-63-0) + 3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol (107010-90-2) → O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol (107035-78-9)

Guidance literature:

With triethylamine; In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1021/ja00257a024

Reference yield:

1,4,7,10,13-pentakis(p-tolylsulfonyl)-1,4,7,10,13-pentaazatridecane (99142-42-4) → O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol (107035-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / K₂CO₃ / dimethylformamide / 60 h / 95 °C

2: 97 percent / Et₃N / CH₂Cl₂ / 1.5 h / Ambient temperature

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja00257a024

Reference yield: 30.0%

1,4,7,10,13-pentakis(p-tolylsulfonyl)-1,4,7,10,13-pentaazatridecane (99142-42-4) + O,O'-bis(methylsulfonyl)-3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol (107035-78-9) → 1,4,7,10,13,16,19,22,25,28-decakis(p-tolylsulfonyl)-1,4,7,10,13,16,19,22,25,28-decaazacyclotriacontane (107010-91-3)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 95 ℃; for 48h;

DOI:10.1021/ja00257a024

upstream raw materials:

methanesulfonyl chloride

3,6,9,12,15-pentakis(p-tolylsulfonyl)-3,6,9,12,15-pentaazaheptadecane-1,17-diol

1,4,7,10,13-pentakis(p-tolylsulfonyl)-1,4,7,10,13-pentaazatridecane

Downstream raw materials:

1,4,7,10,13,16,19,22,25,28-decakis(p-tolylsulfonyl)-1,4,7,10,13,16,19,22,25,28-decaazacyclotriacontane

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