Technology Process of C19H24O5
There total 8 articles about C19H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
chloroform;
at 60 ℃;
for 12.25h;
Inert atmosphere;
DOI:10.1002/asia.201403228
- Guidance literature:
-
With
pyridine;
In
chloroform;
at 60 ℃;
for 12.25h;
Inert atmosphere;
DOI:10.1021/ja108907x
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: toluene-4-sulfonic acid / dichloromethane; water / 7 h / Reflux; Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.15 h / 0 °C / Inert atmosphere
3.1: pyridine / 0 - 20 °C / Inert atmosphere
4.1: sodium ethanolate / ethanol / 48 h / Inert atmosphere; Reflux
5.1: toluene-4-sulfonic acid / acetone / 4 h / 0 - 20 °C / Inert atmosphere
6.1: sodium hydride / mineral oil; tetrahydrofuran / 1.25 h / 0 °C / Inert atmosphere
6.2: 4.5 h / 0 °C / Inert atmosphere; Reflux
7.1: pyridine / chloroform / 12.25 h / 60 °C / Inert atmosphere
With
pyridine; lithium aluminium tetrahydride; sodium ethanolate; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; water; acetone; mineral oil;
DOI:10.1002/asia.201403228