3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene

Base Information

• Chemical Name: 3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene
• CAS No.: 135715-19-4
• Molecular Formula: C₂₉H₂₄O₂S₂
• Molecular Weight: 468.64
• Mol file: 135715-19-4.mol

Synonyms:3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene

Chemical Property of 3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene

Chemical Property:

Purity/Quality:

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Technology Process of 3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene

There total 1 articles about 3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

bis(p-tolylsulfonyl)diazomethane (14159-45-6) + Biphenyl-2-yl-(2,4,6-trimethyl-phenyl)-methanethione (113449-38-0) → 3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene (135715-19-4) + 3-Mesityl-4-phenyl-1-tosylbenzothiophene (135715-20-7)

Guidance literature:

With copper acetylacetonate; In benzene; at 80 ℃; for 38h; Mechanism;

Reference yield: 79.0%

3-(Biphenyl-2-yl)-4,6-dimethyl-1-tosylbenzothiophene (135715-19-4) → Biphenyl-2-ylmesitylmethane (135715-21-8)

Guidance literature:

With nickel; In ethanol; benzene; for 32h; Heating;

upstream raw materials:

bis(p-tolylsulfonyl)diazomethane

Biphenyl-2-yl-(2,4,6-trimethyl-phenyl)-methanethione

Downstream raw materials:

Biphenyl-2-ylmesitylmethane

Refernces