2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

Base Information

Chemical Name:2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:
CAS No.:852949-00-9
Molecular Formula:C₂₀H₂₇O₅P
Molecular Weight:378.405
Hs Code.:

Synonyms:2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

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Chemical Property of 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

Chemical Property:

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Technology Process of 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

There total 5 articles about 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid: which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852949-01-0
diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

: 852949-00-9
2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

Guidance literature:: With trimethylsilyl bromide;

Reference yield:

: 322472-55-9
3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)benzaldehyde

: 852949-00-9
2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: hydrogen / palladium on activated charcoal / ethanol; acetic acid / 5 h

3.1: trimethylsilyl bromide

With trimethylsilyl bromide; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetic acid;

Reference yield:

: 852948-93-7
diethyl trans-2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]vinylphosphonate

: 852949-00-9
2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonic acid:

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on activated charcoal / ethanol; acetic acid / 5 h

2: trimethylsilyl bromide

With trimethylsilyl bromide; hydrogen; palladium on activated charcoal; In ethanol; acetic acid;